Both OIML and NIST Handbook (including latest USP 41 updates) accuracy classes are supported. That way it is easier to be sure that the load’s center of gravity is in the specified location. Sometimes the results of a weighing instrument can vary slightly depending if the load is placed in different locations on the load receptor. In this article, I look at the practical considerations and the different tests you should perform when calibrating your weighing scales/instruments. For a multi-range instrument, a load close but below the first range max is often sufficient. Set the loads of the first test point, wait for stabilization, and record the indication. endobj Even instrument’s zero and full range are adjusted correctly, there is error in the midrange due to unlinearity of the instrument: Hysteresis is the difference in the indication when a test point is approached with increasing or decreasing weight. You should find out the technical characteristics of the weighing instrument (max weight, d value), the accuracy requirement (max error allowed and uncertainty) and what to do if the calibration fails (adjustment). He started working for Beamex in 1988 and has, during his years at Beamex, worked in production, the service department, the calibration laboratory, as quality manager, as product manager and as product marketing manager. %���� x�u�1O�0����[ �!%�Vڌ�����:�Qb��U����0�[��;�}����ir\C�"�� �B4Mb`� O�>[�5�QFvh���*G��tc|-�����߻a���F�V괞�����&��(�xo��r�����޵��Y�]�a�:h�2uUb�.��. Weighing in the Pharmaceutical Industry T Scorer, M Perkin, M Buckley Measurement Good Practice Guide No. x�+� � | Generally, the test points are selected so that they are equally distributed throughout the range. The calibration applies for the current ambient temperature. As the aim of the eccentricity test is to find out the difference caused by the location of the load, it is not necessary to have an accurate calibrated load. 3. 3 0 obj<> 7 0 obj<> number of decimal places over the whole operating range. As with any measurement instruments, weighing instruments should also be calibrated regularly to assure that they are measuring correctly and accurately. Drift check. balance has an on-board calibration function. endobj balance is used or whether calibration of a limited range is desired; this could improve the uncertainty assigned to the balance for the limited range. Internet: www.oiml.org . SOP No. c. When weighing, apply load to center of balance. The balance would come in the weighing mode. 4 0 obj<> The load does not necessarily need to be a calibrated load, as the aim is to find out the repeatability. Wait till zero reading is displayed on the screen. EQ-03-08 Date Revised 02-03-17 Page 5 of 6 . 5.7.4 Message of CAL DONE would be displayed on the screen. 12 0 obj <>stream Many weighing instruments are used for legal measurements or measurements used as basis for monetary transfer and these are part of a legal or statutory verification program based on legislation. Calibration Procedure for Analytical Balances and Scales. Industries for weighing wide range of substances accurately. The load used should be close to the maximum load of the instrument. The indication is zeroed before the test. Ankur Choudhary Print Question Forum 13 comments CALIBRATION OF TOP PAN BALANCE Calibration procedure Internal calibration It shall be performed as per the manufacturer’s instructions. as needed. [>��������,��e�n�������R�.te�M&1n-�w��Q�N��ip��Ń�F췳� ����#�+�+6�x��Ɍ�/x���-�� Lz�D[g�ٯ�-�^U�-y'�j�h�M���ﾲpJGS����,�C��3�� W�6�ԋ�D�V\��:ʛ�����y��F�����{E�Y{�$MY��J�?��/�~�tu�+�r��7'#v��C*YGm�VT��JҿHA�lw�Vxd�(����A�x�����f��*�myu1��>�?�o. Alternatively, you may also tare the instrument when the load is in location number 1, as this makes it easier to see any difference between locations. 7. (error) within which a balance or scale is acceptable for mostsoillaboratory applications. With multi-range instruments, each range is to be calibrated separately. A proper metrologically traceable calibration is the only way to know how accurately weighing instruments are measuring. Heikki has a Bachelor’s degree in Science. Some weighing instruments are small laboratory instruments measuring a few grams and are very accurate. If possible, the load used should be a single load (not several small loads). Additional information on OIML Publications may be obtained from the Organization’s headquarters: Bureau International de Métrologie Légale . Heikki's family consists of himself, his wife and their four children. This test is anyhow required within some industries, like the pharmaceutical industry. Continue increasing the loads through all the increasing test points. endobj endstream Before weighing or calibration, the balance should exactly in a horizontal position (check the level indicator, which should be in the center). Estimates of Uncertainty of the Calibration of Balances Chart 1 shows the uncertainty (estimates) of the calibration of representative electronic balances. endobj 1. Often a repeatability test is done with one load only, but it can be done also with several different load values separately. Before you can start the calibration of the weighing instrument, you should clarify a few things and get prepared. Make sure you have enough weights for the calibration procedure available. Each balance has a built-in calibration system. The zero may be checked between each location to see that it has not changed. If suitable testing facilities for the calibration … Posted January 16, 2020 by Kevin Hill & filed under analytical balances.. Use multiple smaller weights for checking larger weight measurements if necessary. endobj Zero the balance by pressing the “tare” bar (or button) 6. When instrument is calibrated, the results are different with increasing and decreasing calibration points: Minimum weight test is a test that is not always required to be done. Scope: Applicable to all weighing balances except analytical balances. E-mail: biml@oiml.org . 11, rue Turgot - 75009 Paris - France . In order to test how much effect the location of the load has, the eccentricity test is performed. What information should the calibration certificate include. When the measured value gets smaller, typically the relative error of the reading becomes higher. More test points can be used for the typical range of usage of the instrument. MONTHLY CALIBRATION Set the standard weights for various balances based on the capacity of the balance as mentioned in table – I. 8 0 obj <>stream Picture below is a general illustration of hysteresis. The weighing instrument should be at a horizontal level, especially for small and accurate weighing instruments. Correct it by turning leveling feet until the level bubble is in the center of the indicator. Update February 2019: We made an educational video on weighing scale calibration, you can find that in this link: Weighing Scale Calibration Video . 3. If it is required, remember to zero/tare the scale after turning the scale on for the most accurate measurement. x�+� � | Then the load is placed again, and so on. The test load is placed to location 1 and indication is recorded. In the eccentricity test, the reference load is placed in a few different specified locations on the load receptor. 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